AS 2678.2-2008

AS 2678.2-2008

Zinc sulfide concentrates - Chemical analysis Determination of zinc - Ion-exchange/EDTA titrimetric method

Standards Australia

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Table of Contents

<toc>
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<pageno>1</pageno>
<text>AS 2678.2-2008 Zinc sulfide concentrates-Chemical analysis - Part 2: Determination of zinc-Ion-exchange/EDTA titrimetric method</text>
<bookmark index=&apos;1&apos;>
<pageno>4</pageno>
<text>PREFACE</text>
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<bookmark index=&apos;2&apos;>
<pageno>5</pageno>
<text>CONTENTS</text>
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<bookmark index=&apos;3&apos;>
<pageno>7</pageno>
<text>1 Scope</text>
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<bookmark index=&apos;4&apos;>
<pageno>7</pageno>
<text>2 Normative references</text>
</bookmark>
<bookmark index=&apos;5&apos;>
<pageno>7</pageno>
<text>3 Principle</text>
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<bookmark index=&apos;6&apos;>
<pageno>7</pageno>
<text>4 Reagents</text>
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<bookmark index=&apos;7&apos;>
<pageno>9</pageno>
<text>5 Apparatus</text>
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<bookmark index=&apos;8&apos;>
<pageno>9</pageno>
<text>6 Sample</text>
<bookmark index=&apos;9&apos;>
<pageno>9</pageno>
<text>6.1 Test sample</text>
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<bookmark index=&apos;10&apos;>
<pageno>9</pageno>
<text>6.2 Test portion</text>
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<bookmark index=&apos;11&apos;>
<pageno>9</pageno>
<text>7 Procedure</text>
<bookmark index=&apos;12&apos;>
<pageno>9</pageno>
<text>7.1 Number of determinations</text>
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<pageno>10</pageno>
<text>7.2 Blank test</text>
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<pageno>10</pageno>
<text>7.3 Dissolution of test portion</text>
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<bookmark index=&apos;15&apos;>
<pageno>10</pageno>
<text>7.4 Preparation of the ion-exchange column</text>
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<bookmark index=&apos;16&apos;>
<pageno>11</pageno>
<text>7.5 Adsorption of zinc on ion-exchange column</text>
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<pageno>11</pageno>
<text>7.6 Elution of zinc from ion-exchange column</text>
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<pageno>11</pageno>
<text>7.7 Titration</text>
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<bookmark index=&apos;19&apos;>
<pageno>11</pageno>
<text>7.8 Determination of the titration factor of the EDTA standard volumetric solution</text>
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<pageno>12</pageno>
<text>8 Expression of results</text>
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<bookmark index=&apos;21&apos;>
<pageno>13</pageno>
<text>9 Precision</text>
<bookmark index=&apos;22&apos;>
<pageno>13</pageno>
<text>9.1 Expression of precision</text>
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<bookmark index=&apos;23&apos;>
<pageno>13</pageno>
<text>9.2 Procedure for obtaining the final result</text>
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<bookmark index=&apos;24&apos;>
<pageno>13</pageno>
<text>9.3 Between-laboratories precision</text>
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<bookmark index=&apos;25&apos;>
<pageno>14</pageno>
<text>9.4 Check of trueness</text>
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<bookmark index=&apos;26&apos;>
<pageno>15</pageno>
<text>10 Test report</text>
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<bookmark index=&apos;27&apos;>
<pageno>16</pageno>
<text>Annex A (normative) Ion-exchange resins and columns</text>
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<bookmark index=&apos;28&apos;>
<pageno>18</pageno>
<text>Annex B (normative) Procedure for the preparation and determination of the mass of a predried test portion</text>
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<bookmark index=&apos;29&apos;>
<pageno>20</pageno>
<text>Annex C (normative) Determination of cadmium by atomic absorption spectrometry</text>
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<bookmark index=&apos;30&apos;>
<pageno>22</pageno>
<text>Annex D (normative) Flowchart of the procedure for the acceptance of analytical values for test samples</text>
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<bookmark index=&apos;31&apos;>
<pageno>23</pageno>
<text>Annex E (informative) Effect of potentially interfering elements</text>
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<bookmark index=&apos;32&apos;>
<pageno>24</pageno>
<text>Annex F (informative) Derivation of precision equations</text>
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<bookmark index=&apos;33&apos;>
<pageno>29</pageno>
<text>Bibliography</text>
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</toc>

Abstract

Adopts ISO 12739:2006 to provide determination of zinc in zinc sulphide concentrates by an ion-exchange/EDTA titrimetric method.

General Product Information

Document Type Standard
Status Current
Publisher Standards Australia
Committee MN-005
Supersedes
  • DR 07036 CP
  • AS 2678.2-1999

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