API 4713 : 2002

TEST REPORT: FLUIDIZED CATALYTIC CRACKING UNIT AT A REFINERY (SITE A) - CHARACTERIZATION OF FINE PARTICULATE EMISSION FACTORS AND SPECIATION PROFILES FROM STATIONARY PETROLEUM INDUSTRY COMBUSTION SOURCES

American Petroleum Institute

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ACKNOWLEDGMENTS
EXECUTIVE SUMMARY
FINDINGS
1.0 PROJECT DESCRIPTION
      PROJECT OVERVIEW
      PROJECT OBJECTIVES
        Primary Objectives
        Secondary Objectives
      TEST OVERVIEW
        Source Level (In-Stack) Samples
        Dilution Stack Gas Samples
        Process Samples
      KEY PERSONNEL
2.0 PROCESS DESCRIPTION
      SAMPLING LOCATIONS
3.0 TEST PROCEDURES
      STACK GAS FLOW RATE, MOISTURE CONTENT AND MOLECULAR WEIGHT
      O[2], CO[2], CO, NO[x] AND SO[2]
      IN-STACK METHOD TESTS
        In-Stack Total Filterable PM, PM10 and PM2.5
        Particle Size Distribution
        Condensible Particulate Matter Mass and Chemical Analysis
        SO[3] and NH[3]
      DILUTION TUNNEL TESTS
      PM2.5 Mass
        Elements
        Sulfate, Nitrate, Chloride and Ammonium Emissions
        Organic and Elemental Carbon
        Volatile Organic Compounds
        Semivolatile Organic Compounds
4.0 TEST RESULTS
      PROCESS OPERATING CONDITIONS
      PRELIMINARY TEST RESULTS
      STACK CONDITIONS AND FLOW RATE
      CO, NO[x] AND SO[2] EMISSIONS
      IN-STACK AND IMPINGER METHOD RESULTS
        Particulate Mass
        Particle Size Distribution
        OC, EC, and SVOCs (In-Stack Filters)
        SO[3] and NH[3]
      DILUTION TUNNEL RESULTS
        Particulate Mass
        SO[4], NO[3], Cl and NH[4]
        OC, EC and Organic Species
        Elements
      PROCESS SAMPLES
        ESP Fines
        Spent and Regenerated Catalyst Samples
5.0 EMISSION FACTORS AND SPECIATION PROFILES
      IN-STACK AND IMPINGER METHOD RESULTS
      DILUTION TUNNEL RESULTS
6.0 QUALITY ASSURANCE
      DILUTION TUNNEL QA/QC RESULTS
        Dilution Tunnel Flows
        Blank Results - Dilution Tunnel
        QA Checks - Dilution Tunnel Particulate Mass
        Precision - Dilution Tunnel
      IN-STACK AND IMPINGER METHOD QA/QC RESULTS
        CEMS Analysis
      PROCESS SAMPLE QA/QC RESULTS
      ANALYTICAL QA/QC PROCEDURES
        Particulate Mass
        Elemental (XRF) Analysis
        Organic and Elemental Carbon Analysis
        Sulfate, Nitrate, Chloride and Ammonium Analysis
        SVOC Analysis
        VOC Analysis
      SAMPLE STORAGE AND SHIPPING
7.0 DISCUSSION AND FINDINGS
      PRIMARY PM2.5 MASS EMISSIONS
      PARTICLE SIZE DISTRIBUTION
      SPECIATION OF PRIMARY PM2.5 EMISSIONS
      PM2.5 PRECURSOR EMISSIONS
      FINDINGS
REFERENCE
Appendix A - GLOSSARY
Appendix B - SI CONVERSION FACTORS